1H NMR (DMSO-d6) and 19F NMR (DMSO-d6) Spectroscopic and Mass Spectrometric Analysis
Identification (Mass Spectrometry)
Matches structure
Complies
NMR
Matches structure
Complies
Purity (TLC)
98%
Atmosphere
Air
Melting Point
130-134 °C
Solubility
DMSO, Methanol
Specific Rotation
-24.27 °
Carbon Content
48.95%
Hydrogen Content
5.37%
Nitrogen Content
4.59%
TEST CONDITIONS
TLC Conditions: SiO2: Dichloromethane : Methanol = 9 : 1; Visualized with UV and KMnO4; Rf=0.35.Specific Rotation Conditions: c=0.50, Chloroform
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